This episode describes the development of an autonomous laboratory that uses mobile robots to automate chemical discovery processes, simulating human decisions in exploratory chemistry. The system incorporates analytical tools and robots to synthesize, analyze, and assess chemical compounds, paving the way for new applications in areas such as drug discovery, supramolecular synthesis, and photocatalysis. The autonomous laboratory has proven effective in managing a wide range of complex reactions with high efficiency and reproducibility, opening new perspectives for chemical research and industry.